3-乙氧基硫代羰基氨磺酰苯基乙酸合成路线 （共 3 条）
反应条件
sodium hydroxide in water 5 h; Heating;
参考文献
GLAXO GROUP LIMITED; WANG, Yonghui; YANG, Ting; LIU, Qian; XIANG, Jia-Ning
Patent: WO2012/28100 A1, 2012 ;
Location in patent: Page/Page column 29-30 ;
WO 2012/028100 A1
反应条件
hydrogenchloride; sodium nitrite
1.) H2O, 2.) 60 deg C, 90 deg C, 0.5 h; Multistep reaction;
参考文献
Collman, James P.; Groh, Susan E.
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1391 - 1403
反应条件
1: 70 percent / FeSO4-7H2O, NH4OH / H2O / 0.17 h / Heating; pH 10
2: 1.) sodium nitrite, HCl / 1.) H2O, 2.) 60 deg C, 90 deg C, 0.5 h
View Scheme
参考文献
Collman, James P.; Groh, Susan E.
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1391 - 1403
