6-羟基-5,10-二甲氧基-7H-二苯并[De,h]喹啉-7-酮合成路线 （共 6 条）
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
反应条件
1: 81.9 percent / 10percent aq. NaOH / diethyl ether / 1 h / 0 - 5 °C
2: 54.2 percent / POCl3 / toluene / 2.5 h / 120 °C
3: 70.9 percent / dimethylformamide / 5 h / 180 °C
4: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating
5: 64.1 percent / polyphosphoric acid / 1 h / 100 °C
View Scheme
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
反应条件
1: 70.9 percent / dimethylformamide / 5 h / 180 °C
2: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating
3: 64.1 percent / polyphosphoric acid / 1 h / 100 °C
View Scheme
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
反应条件
1: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating
2: 64.1 percent / polyphosphoric acid / 1 h / 100 °C
View Scheme
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
反应条件
1: 54.2 percent / POCl3 / toluene / 2.5 h / 120 °C
2: 70.9 percent / dimethylformamide / 5 h / 180 °C
3: 41.1 percent / H2O/KOH / bis-(2-hydroxy-ethyl) ether / 24 h / Heating
4: 64.1 percent / polyphosphoric acid / 1 h / 100 °C
View Scheme
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
反应条件
silver(l) oxide in methanol; chloroform
T=60°C; 6 h;
参考文献
Kunitomo, J.; Satoh, M.; Shingu, T.
Tetrahedron, 1983 , vol. 39, # 20 p. 3261 - 3266
