1: With dimethylsulfide borane complex in tetrahydrofuran
T=0 - 70°C;
2: With hydrogenchloride; water in tetrahydrofuran
T=0°C; 0.583333 h; Heating / reflux;
3: With sodium hydrogencarbonate in tetrahydrofuran; water
参考文献
Millennium Pharmaceuticals, Inc.
Patent: US2008/171754 A1, 2008 ;
Location in patent: Page/Page column 105 ;
US 20080171754 A1