3,4-二氢-2H-喹噁啉-1-羧酸叔丁酯合成路线 (共 3 条)
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in tetrahydrofuran T=80°C; 18 h;
参考文献
Jangili, Paramesh; Kashanna, Jajula; Das, Biswanath
Tetrahedron Letters, 2013 , vol. 54, # 26 p. 3453 - 3456
反应条件
sodium hydroxide in tetrahydrofuran T=20°C; Cooling with ice;
参考文献
EP2172453 A1, ;
Page/Page column 17 ;
EP 2172453 A1
反应条件
1: sodium hydride / N,N-dimethyl-formamide 2: copper(l) iodide; N-methyl-2-(methylamino)ethylamine; caesium carbonate / tetrahydrofuran / 18 h / 80 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 26 p. 3453 - 3456