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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88766-28-3
合成路线
(共 20 条)
87463-08-9
→
反应条件
26555-39-5
+
26555-41-9
+
88766-27-2
+
88766-28-3
反应条件
potassium iodide in water T=0°C; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
34520-64-4
→
反应条件
26555-41-9
+
88766-27-2
+
88766-28-3
反应条件
disulfur dichloride in diethyl ether 1.) 0 deg C, 2.) 25 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
1115-13-5
→
反应条件
26555-41-9
+
88766-27-2
+
88766-28-3
反应条件
disulfur dichloride 1.) dry ice cooling, 2.) 25 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
1115-13-5
→
反应条件
26555-41-9
+
88766-28-3
+
88766-25-0
反应条件
tetrasulfur dichloride 1.) dry ice cooling, 2.) 25 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
1115-13-5
→
反应条件
26555-41-9
+
88766-27-2
+
88766-28-3
+
88766-25-0
反应条件
trisulfur dichloride 1.) dry ice cooling, 2.) 25 deg C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
26555-40-8
氯化甲氧羰基硫
→
反应条件
26555-41-9
+
88766-27-2
+
88766-28-3
+
88766-25-0
反应条件
monodisulfide in dichloromethane T=25°C; 2 h; Product distribution;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
87463-08-9
→
反应条件
26555-39-5
+
26555-41-9
+
88766-27-2
+
88766-28-3
+
88766-25-0
反应条件
sodium iodide in water T=0°C; Product distribution;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
26555-40-8
氯化甲氧羰基硫
→
反应条件
26555-39-5
+
26555-41-9
+
88766-27-2
+
88766-28-3
+
88766-25-0
+
88766-31-8
反应条件
sodium sulfide in chloroform; water T=25°C; 4 h; Product distribution;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
88766-29-4
→
反应条件
26555-41-9
+
88766-27-2
+
88766-28-3
+
88766-25-0
+
88766-31-8
反应条件
ethanol 3 h; Product distribution;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
26555-40-8
氯化甲氧羰基硫
→
反应条件
26555-39-5
+
26555-41-9
反应条件
ethanol T=0°C; 14 h; Product distribution;
参考文献
Barany, George; Mott, Andrew W.
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1043 - 1051
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