2-(2-甲氧基乙氧基)乙硫醇合成路线 (共 2 条)
反应条件
1: With thiourea in ethanol
3 h; Heating;
2: With sodium hydroxide
3.75 h; Heating;
参考文献
Snow, Arthur W.; Foos, Edward E.
Synthesis, 2003 , # 4 p. 509 - 512
反应条件
1.1: 84 percent / pyridine / 12 h / 0 °C
2.1: 33 percent aq. Na2CS3; CS2 / 5 h / 65 °C
2.2: 75 percent / H2SO4
View Scheme
参考文献
Yanic, Cemile; Bredenkamp, Martin W.; Jacobs, Edmund P.; Swart, Pieter
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 7 p. 1381 - 1384