(2E)-1-(2-羟基苯基)-3-苯基-2-丙烯-1-酮合成路线 （共 83 条）
反应条件
1: 86 percent / Pd(PPh3)2Cl2; CuI; Et3N / dimethylformamide / 24 h / 20 °C
2: 73 percent / p-toluenesulfonic acid / benzene / 24 h / 20 °C
View Scheme
参考文献
De, Mahuya; Majumdar, Dyuti P.; Kundu, Nitya G.
Journal of the Indian Chemical Society, 1999 , vol. 76, # 11-12 p. 665 - 674
反应条件
1: palladium diacetate; dipotassium peroxodisulfate; trifluoroacetic acid; trifluoroacetic anhydride / 12 h / 50 °C / |Sealed tube
2: sodium hydroxide / ethanol / 12 h / 20 °C
View Scheme
参考文献
Shan, Gang; Yang, Xinglin; Ma, Linlin; Rao, Yu
Angewandte Chemie - International Edition, 2012 , vol. 51, # 52 p. 13070 - 13074
Angew. Chem., 2012 , vol. 124, # 52 p. 13247 - 13251,5
反应条件
in 1,4-dioxane; water
T=30°C; pH range: 8-11, equilibrium; Rate constant;
参考文献
Old, K. Barry; Main, Lyndsay
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1309 - 1312
反应条件
in acetonitrile
3 h; Ambient temperature;
参考文献
Patonay, Tamas; Patonay-Peli, Erzsebet; Litkei, Gyoergy
Tetrahedron, 1987 , vol. 43, # 8 p. 1827 - 1834
反应条件
dimethyl sulfoxide
120 h; Ambient temperature;
参考文献
Reddy, Jagannadha N.; Pawar, Sevak Ram; Sharma, Tarachand
Journal of Chemical and Engineering Data, 1986 , vol. 31, # 3 p. 377 - 379
反应条件
pyrimidolt;5,4-ggt;pteridine N-oxide deriv in acetonitrile
0.833333 h; Ambient temperatureIrradiation; Product distributionMechanism;
参考文献
Maki, Yoshifumi; Shimada, Kaoru; Sako, Magoichi; Hirota, Kosaku
Tetrahedron, 1988 , vol. 44, # 11 p. 3187 - 3194
反应条件
dimethyl sulfoxide
3 h; Heating; Further byproducts given;
参考文献
Reddy, Jagannadha N.; Pawar, Sevak Ram; Sharma, Tarachand
Journal of Chemical and Engineering Data, 1986 , vol. 31, # 3 p. 377 - 379
反应条件
in benzene
26 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Patonay, Tamas; Patonay-Peli, Erzsebet; Litkei, Gyoergy
Tetrahedron, 1987 , vol. 43, # 8 p. 1827 - 1834
反应条件
sodium lauryl sulfate in water
6 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Singh, A.K.; Raghuraman, T.S.
Tetrahedron Letters, 1985 , vol. 26, # 34 p. 4125 - 4128
反应条件
sodium hydroxide; water
参考文献
Dhar, Durga N.; Bag, Amal K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 627 - 631
