(2E)-1-(2-羟基苯基)-3-苯基-2-丙烯-1-酮合成路线 (共 83 条)
反应条件
Flash photolysis; Quantum yield;
参考文献
Norikane, Yasuo; Itoh, Hiroki; Arai, Tatsuo
Chemistry Letters, 2000 , # 9 p. 1094 - 1095
反应条件
triethanolamine
0.25 h; Heating;
参考文献
Agrawal, Nitin N.; Soni
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 12 p. 2700 - 2701
反应条件
dicyclohexyl-carbodiimide in methanol
Irradiation;
参考文献
Pandey, G.; Krishna, A.; Kumaraswamy, G.
Tetrahedron Letters, 1987 , vol. 28, # 39 p. 4615 - 4616
反应条件
1: sodium hydroxide; dihydrogen peroxide / ethanol / 20 °C
2: potassium carbonate / acetone / 24 h / |Reflux
View Scheme
参考文献
Juvale, Kapil; Stefan, Katja; Wiese, Michael
European Journal of Medicinal Chemistry, 2013 , vol. 67, p. 115 - 126
反应条件
dicyclohexyl-carbodiimide
Irradiation;
参考文献
Pandey, G.; Krishna, A.; Kumaraswamy, G.
Tetrahedron Letters, 1987 , vol. 28, # 39 p. 4615 - 4616
反应条件
1: 77 percent / toluene / 4 h / Heating
2: 58 percent / 30percent H2O2, 2N NaOH / ethanol
View Scheme
参考文献
Dhar, Durga N.; Bag, Amal K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 627 - 631
反应条件
1: 77 percent / toluene / 4 h / Heating
2: 86 percent / Br2 / CHCl3
View Scheme
参考文献
Dhar, Durga N.; Bag, Amal K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 7 p. 627 - 631
反应条件
1: bromoacetic acid N-hydroxysuccinimide ester; triphenylphosphino resin in toluene
16 h;
2: With triethylamine in dichloromethane
16 h;
3: 3-phenyl-1-(2-hydroxyphenyl)-prop-2-ene-1-one in 1,4-dioxane
T=180°C; 0.25 h; microwave irradiation; Further stages.;
参考文献
Henkel, Bernd
Synlett, 2008 , # 3 p. 355 - 358
反应条件
in toluene
24 h; Heating;
参考文献
Joshi, U. K.; Kelkar, R. M.; Paradkar, M. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 11 p. 1151 - 1152
反应条件
sodium borohydride; R-toluene sulfonic acid; hydrogen; palladium monocarbide in ethanol; acetic acid
参考文献
Batchelor; John F.; Bauer; Denis J.; Hodson; Harold F.; Selway; John W. T.; Young; David A. B.
Patent: US4461907 A1, 1984 ;