3,5-二苯基-1,2,4-恶二唑合成路线 （共 159 条）
反应条件
T=140°C; 0.0333333 h; Microwave irradiationSealed vessel;
参考文献
Neves Filho, Ricardo Antonio Wanderley; Da Silva, Cecilia Aguiar; Da Silva, Clecia Sipriano Borges; Brustein, Vanessa Passos; Navarro, Daniela Maria Do Amaral Ferraz; Dos Santos, Fabio Andre Brayner; Alves, Luiz Carlos; Cavalcanti, Marilia Gabriela Dos Santos; Srivastava, Rajendra Mohan; Carneiro-Da-Cunha, Maria Das Gracas
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 8 p. 819 - 825
反应条件
1: 4-methyl-morpholine / 1,4-dioxane / 0.58 h / 20 °C
2: 1,4-dioxane / 3 h / |Reflux
View Scheme
参考文献
Ramu, Tadikonda; Prasanthi, Sarakula; Mangarao, Nakka; Basha, Gajula Mahaboob; Srinuvasarao, Rayavarapu; Siddaiah, Vidavalur
Chemistry Letters, 2013 , vol. 42, # 7 p. 722 - 724
反应条件
ethanol; hydroxylamine hydrochloride
参考文献
Beckmann; Sandel
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 293
反应条件
toluene-4-sulfonic acid; dicyclohexyl-carbodiimide in chloroform
4 h; Heating; Further byproducts given;
参考文献
Kawashima; Tabei
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 6 p. 1657 - 1660
反应条件
toluene-4-sulfonic acid in chloroform
4 h; Heating; Further byproducts given;
参考文献
Kawashima; Tabei
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 6 p. 1657 - 1660
反应条件
triethylamine in benzene
12 h; Heating; Further byproducts given;
参考文献
Blake, Alexander J.; Dawson, Ian M.; Forsyth, Angus C.; Johnson, Trevor; Paton, R. Michael; et al.
Journal of Chemical Research, Miniprint, 1988 , # 10 p. 2548 - 2580
反应条件
1: triethylamine / dichloromethane / 48 h / 20 °C
2: phosphorous acid trimethyl ester / benzene / 2 h / |Reflux
View Scheme
参考文献
Memeo, Misal Giuseppe; Dondi, Daniele; Mannucci, Barbara; Corana, Federica; Quadrelli, Paolo
Tetrahedron, 2013 , vol. 69, # 35 p. 7387 - 7394
反应条件
in acetic acid
8 h; Heating;
参考文献
Leite, Lucia F. C. da Costa; Srivastava, Rajendra M.; Cavalcanti, Alexandre P.
Bulletin des Societes Chimiques Belges, 1989 , vol. 98, # 3 p. 203 - 210
反应条件
dicyclohexyl-carbodiimide in chloroform
4 h; Heating; Further byproducts given;
参考文献
Kawashima; Tabei
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 6 p. 1657 - 1660
反应条件
1: absolute diethyl ether; PCl5 / 0 °C / man giesst auf Eis
2: alcohol; hydroxylamine hydrochloride
View Scheme
参考文献
Beckmann; Sandel
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 293
