3,5-二苯基-1,2,4-恶二唑合成路线 （共 159 条）
反应条件
potassium phosphate; oxygen in N,N-dimethyl-formamide
T=100°C; P=760.051 Torr; 1.5 h; Reagent/catalystSolventTemperature;
参考文献
Zhang, Feng-Lian; Wang, Yi-Feng; Chiba, Shunsuke
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6003 - 6007
参考文献
Chiou, Shishue; Shine, Henry J.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 125 - 128
反应条件
triethylamine in methanol
Irradiation; Yield given;
参考文献
Quadrelli; Mella; Caramella
Tetrahedron Letters, 1999 , vol. 40, # 4 p. 797 - 800
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in 1,4-dioxane
T=95 - 100°C; P=760 Torr; 5 h;
参考文献
Zhou, Tao; Chen, Zhen-Chu
Synthetic Communications, 2002 , vol. 32, # 6 p. 887 - 891
反应条件
potassium fluoride; hydroxylamine hydrochloride
T=100°C; 12 h;
参考文献
Rostamizadeh, Shahnaz; Ghaieni, Hamid Reza; Aryan, Reza; Amani, Ali-Mohammad
Synthetic Communications, 2010 , vol. 40, # 20 p. 3084 - 3092
反应条件
[bis(acetoxy)iodo]benzene in dimethyl sulfoxide
T=100°C; 20 h;
参考文献
Wang, Yi-Feng; Zhang, Feng-Lian; Chiba, Shunsuke
Organic Letters, 2013 , vol. 15, # 11 p. 2842 - 2845
反应条件
diphosphorous tetraiodide in dichloromethane
T=20°C; Beckmann Rearrangement; 2 h;
参考文献
Telvekar, Vikas N.; Takale, Balaram S.
Synthetic Communications, 2013 , vol. 43, # 2 p. 221 - 227,7
反应条件
hydroxylamine hydrochloride; sodium carbonate in water; ethylene glycol
T=195°C; 30 h;
参考文献
Outirite, Moha; Lebrini, Mounim; Lagrenee, Michel; Bentiss, Fouad
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 6 p. 1529 - 1531
反应条件
1: 80 percent / diethyl ether / 48 h / Ambient temperature
2: triethylamine / 48 h / Ambient temperature
3: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
sodium hypochlorite; triethylamine in dichloromethane
T=0°C; 0.75 h;
参考文献
Lee, George A.
Synthesis, 1982 , # 6 p. 508 - 509
