3,5-二苯基-1,2,4-恶二唑合成路线 （共 159 条）
反应条件
triethylamine in methanol
T=25°C; 48 h;
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: triethylamine / 48 h / Ambient temperature
2: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: triethylamine / diethyl ether / 6 h / 0 - 20 °C
2: [bis(acetoxy)iodo]benzene / dimethyl sulfoxide / 20 h / 100 °C
View Scheme
参考文献
Wang, Yi-Feng; Zhang, Feng-Lian; Chiba, Shunsuke
Organic Letters, 2013 , vol. 15, # 11 p. 2842 - 2845
反应条件
1: triethylamine / diethyl ether / 6 h / 0 - 20 °C
2: [bis(acetoxy)iodo]benzene / dimethyl sulfoxide / 20 h / 100 °C
View Scheme
参考文献
Wang, Yi-Feng; Zhang, Feng-Lian; Chiba, Shunsuke
Organic Letters, 2013 , vol. 15, # 11 p. 2842 - 2845
反应条件
ethanol; hydroxylamine hydrochloride
参考文献
Beckmann; Sandel
Justus Liebigs Annalen der Chemie, 1897 , vol. 296, p. 293
反应条件
sodium hydride in tetrahydrofuran
4 h; Ambient temperature;
参考文献
Albini, Franca Marinone; Vitali, Danila; Oberti, Roberta; Caramella, Pierluigi
Journal of Chemical Research, Miniprint, 1980 , # 10 p. 4355 - 4384
反应条件
in methanol
5 h; Irradiation;
参考文献
Quadrelli; Mella; Caramella
Tetrahedron Letters, 1999 , vol. 40, # 4 p. 797 - 800
反应条件
1: NH3 / ethanol
2: toluene
View Scheme
参考文献
Durden,J.A.; Heywood,D.L.
Journal of Organic Chemistry, 1965 , vol. 30, p. 4359 - 4361
反应条件
in benzene
16 h; Heating;
参考文献
Belen'kii, L. I.; Brokhovetskii, D. B.; Krayushkin, M. M.
Tetrahedron, 1990 , vol. 46, # 5 p. 1659 - 1668
反应条件
hydroxylamine hydrochloride; sodium methylate in methanol
48 h; Ambient temperature;
参考文献
Lorente, Antonio; Gamez, Pedro; Mar Contreras, Maria del
Heterocycles, 1994 , vol. 38, # 1 p. 113 - 124
