3,5-二苯基-1,2,4-恶二唑合成路线 （共 159 条）
反应条件
triethylamine in ethanol
var. solv. and conc. of reagent; Yield given. Yields of byproduct given;
参考文献
Caramella, P.; Corsaro, A.; Compagnini, A.; Albini, Marinone F.
Tetrahedron Letters, 1983 , vol. 24, # 40 p. 4377 - 4380
反应条件
benzamidoxime in chloroform
4 h; Heating;
参考文献
Kawashima; Tabei
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 6 p. 1657 - 1660
反应条件
1: benzonitrile With magnesia-supported sodium carbonate; hydroxylamine hydrochloride
0.05 h; Irradiation;
2: benzoyl chloride 0.05 h; Irradiation;
参考文献
Kaboudin, Babak; Saadati, Fariba
Tetrahedron Letters, 2007 , vol. 48, # 16 p. 2829 - 2832
反应条件
1: iPr2NEt / CH2Cl2 / 0 °C
2: 80 percent / n-Bu4NF / tetrahydrofuran / 3 h / 23 °C
View Scheme
参考文献
Gangloff, Anthony R.; Litvak, Joane; Shelton, Emma J.; Sperandio, David; Wang, Vivian R.; Rice, Kenneth D.
Tetrahedron Letters, 2001 , vol. 42, # 8 p. 1441 - 1443
反应条件
1: triethylamine / 48 h / Ambient temperature
2: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: triethylamine / 48 h / Ambient temperature
2: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: 99 percent / diethyl ether / 48 h / Ambient temperature
2: triethylamine / methanol / 48 h / Ambient temperature
3: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: 99 percent / diethyl ether / 48 h / Ambient temperature
2: triethylamine / methanol / 48 h / Ambient temperature
3: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: triethylamine / methanol / 48 h / Ambient temperature
2: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
反应条件
1: triethylamine / methanol / 48 h / Ambient temperature
2: 62 percent / benzhydroximoyl chloride, 9,10-dimethylanthracene, triethylamine / methanol / 48 h / Ambient temperature; other reagents: trimethyl phosphite, p-chlorobenzhydroximoyl chloride
View Scheme
参考文献
Quadrelli, Paolo; Invernizzi, Anna Gamba; Falzoni, Mario; Caramella, Pierluigi
Tetrahedron, 1997 , vol. 53, # 5 p. 1787 - 1796
