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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88802-80-6
合成路线
（共 12 条）
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-64-6
反应条件
thionyl chloride in pyridine T=-50 - -45°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-65-7
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-64-6
反应条件
thionyl chloride in pyridine T=-50 - -45°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-65-7
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-64-6
反应条件
thionyl chloride in pyridine T=-50 - -45°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
3419-66-7
1-叔丁基-1-环己烯
+
88802-63-5
+
88802-65-7
反应条件
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
88802-68-0
反应条件
2: 50 percent / xylene / 69 h / 195 °C 3: diisobutyl-aluminumhydride / hexane; 1,2-dimethoxy-ethane / -78 °C 4: n-Butyllithium / tetrahydrofuran / 5 h View Scheme
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
88802-70-4
反应条件
2: 50 percent / xylene / 69 h / 195 °C 3: diisobutyl-aluminumhydride / hexane; 1,2-dimethoxy-ethane / -78 °C 4: n-Butyllithium / tetrahydrofuran / 5 h 5: 80 percent / 1,2-dimethoxy-ethane / 4 h / 170 °C 6: 45 percent / n-Butyllithium / tetrahydrofuran View Scheme
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
88802-71-5
反应条件
2: 50 percent / xylene / 69 h / 195 °C 3: diisobutyl-aluminumhydride / hexane; 1,2-dimethoxy-ethane / -78 °C 4: n-Butyllithium / tetrahydrofuran / 5 h 5: 80 percent / 1,2-dimethoxy-ethane / 4 h / 170 °C 6: 45 percent / n-Butyllithium / tetrahydrofuran 7: 0.481 g / chloroamine, aq. sodium hydroxide / diethyl ether / 1.33 h / 10 °C View Scheme
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
88802-80-6
→
反应条件
88802-74-8
反应条件
2: 50 percent / xylene / 69 h / 195 °C 3: diisobutyl-aluminumhydride / hexane; 1,2-dimethoxy-ethane / -78 °C 4: n-Butyllithium / tetrahydrofuran / 5 h 5: 80 percent / 1,2-dimethoxy-ethane / 4 h / 170 °C 6: 45 percent / n-Butyllithium / tetrahydrofuran 7: 0.481 g / chloroamine, aq. sodium hydroxide / diethyl ether / 1.33 h / 10 °C 8: 0.265 g / NaOCH3 / methanol / -90 - -85 °C / Irradiation View Scheme
参考文献
Ireland, Robert E.; Dow, William C.; Godfrey, Jollie D.; Thaisrivongs, Suvit
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1001 - 1013
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