2-氧代-2-(2-氧代丙基氨基)乙酸乙酯合成路线 (共 2 条)
反应条件
Dess-Martin periodane in dichloromethane
T=20°C; 1 h;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1813603 A1, 2007 ;
Location in patent: Page/Page column 37 ;
EP 1813603 A1
反应条件
1: With trichlorophosphate
0.5 h; Heating / reflux;
2: With potassium carbonate in water; ethyl acetate
T=0°C; pH=9; 0.5 h;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1813603 A1, 2007 ;
Location in patent: Page/Page column 38 ;
EP 1813603 A1