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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88818-33-1
合成路线
（共 12 条）
88818-32-0
→
反应条件
88818-33-1
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 0.5 h; Ambient temperature;
参考文献
Tanoue, Yasuhiro; Terada, Akira
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 6 p. 2039 - 2046
88818-32-0
→
反应条件
88818-33-1
反应条件
ammonium cerium(IV) nitrate
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
10075-68-0
→
反应条件
88818-33-1
反应条件
1: 99 percent / POCl3 / CHCl3 / 6 h / Heating 2: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 3: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 4: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 5: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-38-6
→
反应条件
88818-33-1
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 6: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-28-4
1,4,5,8-四甲氧基萘-2-甲醛
→
反应条件
88818-33-1
反应条件
1: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 2: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 3: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 4: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
15013-16-8
5,8-二甲氧基-1,4-萘二酮
→
反应条件
88818-33-1
反应条件
1: 48 percent / 40percent NaOH, Na2S2O4 / methanol; H2O / 8 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 6: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
10075-63-5
1,5-二甲氧基萘
→
反应条件
88818-33-1
反应条件
1: 58 percent / Br2 / CCl4 / 0.5 h / 70 °C 2: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 3: 99 percent / POCl3 / CHCl3 / 6 h / Heating 4: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 5: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 6: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 7: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-40-0
→
反应条件
88818-33-1
反应条件
1: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 2: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-39-7
→
反应条件
88818-33-1
反应条件
1: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 2: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 3: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
83-56-7
1,5-二羟基萘
→
反应条件
88818-33-1
反应条件
1: 78 percent / NaOH / methanol / 3 h / Heating 2: 58 percent / Br2 / CCl4 / 1 h / 73 - 74 °C 3: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 4: 99 percent / POCl3 / CHCl3 / 10 h / Heating 6: 85 percent / ammonium cerium(IV) nitrate View Scheme
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
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