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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88818-34-2
合成路线
（共 14 条）
106395-86-2
→
反应条件
88818-34-2
反应条件
sodium hydroxide T=0 - 5°C; 5 h;
参考文献
Tanoue, Yasuhiro; Terada, Akira; Sugyoe, Yasunari
Journal of Organic Chemistry, 1987 , vol. 52, # 8 p. 1437 - 1439
88818-33-1
→
反应条件
88818-34-2
反应条件
argentic oxide; nitric acid
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-30-8
→
反应条件
88818-34-2
反应条件
argentic oxide; nitric acid in acetone 0.5 h; Ambient temperature;
参考文献
Tanoue, Yasuhiro; Terada, Akira
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 6 p. 2039 - 2046
10075-68-0
→
反应条件
88818-34-2
反应条件
1: 99 percent / POCl3 / CHCl3 / 6 h / Heating 2: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 3: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 4: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 5: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 6: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-38-6
→
反应条件
88818-34-2
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 6: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 7: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-28-4
1,4,5,8-四甲氧基萘-2-甲醛
→
反应条件
88818-34-2
反应条件
1: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 2: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 3: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 4: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 5: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-32-0
→
反应条件
88818-34-2
反应条件
1: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 2: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
15013-16-8
5,8-二甲氧基-1,4-萘二酮
→
反应条件
88818-34-2
反应条件
1: 48 percent / 40percent NaOH, Na2S2O4 / methanol; H2O / 8 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 6: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 7: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
10075-63-5
1,5-二甲氧基萘
→
反应条件
88818-34-2
反应条件
1: 58 percent / Br2 / CCl4 / 0.5 h / 70 °C 2: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 3: 99 percent / POCl3 / CHCl3 / 6 h / Heating 4: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 5: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 6: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 7: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 8: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-40-0
→
反应条件
88818-34-2
反应条件
1: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 2: 70 percent / cerium(IV) ammonium nitrate / CHCl3; acetonitrile; H2O / 0.17 h / Ambient temperature 3: 27 percent / AgO, 40percent HNO3 / acetone / 0.17 h / Ambient temperature View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
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