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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88818-38-6
合成路线
（共 14 条）
88818-38-6
→
反应条件
475-38-7
萘茜
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 68 percent / BBr3 / CH2Cl2 / 2 h / -70 °C View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-38-6
+
124-41-4
甲醇钠
→
反应条件
10075-68-0
反应条件
copper(l) iodide in methanol; N,N-dimethyl-formamide 36 h; Reflux;
参考文献
Wang, Rubing; Zheng, Xiaogang; Zhou, Wen; Peng, Ying; Zhu, Mengyuan; Li, Shaoshun
Journal of Chemical Research, 2010 , # 9 p. 520 - 521
88818-38-6
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
128038-44-8
1,5-二甲酰基-4,8-二甲氧基萘
反应条件
n-butyllithium 1.) THF, from -70 deg C to -65 deg C, 2.) THF, from -70 deg C to -60 deg C; Yield given. Multistep reaction;
参考文献
Sylvester-Hvid; Sorensen; Schaumburg; Bechgaard; Christensen
Synthetic Communications, 1993 , vol. 23, # 13 p. 1905 - 1914
10075-63-5
1,5-二甲氧基萘
→
反应条件
88818-38-6
反应条件
N-bromosuccinmide in tetrachloromethane T=20°C; 8 h;
参考文献
Carreno, M. Carmen; Ruano, Jose L. Garcia; Sanz, Gema; Toledo, Miguel A.; Urbano, Antonio
Journal of Organic Chemistry, 1995 , vol. 60, # 16 p. 5328 - 5331
83-56-7
1,5-二羟基萘
→
反应条件
88818-38-6
反应条件
1: 78 percent / NaOH / methanol / 3 h / Heating 2: 58 percent / Br2 / CCl4 / 1 h / 73 - 74 °C View Scheme
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
56-23-5
四氯化碳
+
10075-63-5
1,5-二甲氧基萘
+
7726-95-6
溴
→
反应条件
88818-38-6
反应条件
暂无反应条件数据
参考文献
Carter et al.
Journal of the Chemical Society, 1942 , p. 236,239
88818-38-6
→
反应条件
77386-93-7
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 1.) 60percent NaH, 2.) p-toluenesulfonic acid monohydrate / 1.) THF, r.t., overnight, 2.) acetone, 0-5 deg C, 3 h 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature 6: 104 mg / SOCl2 / pyridine / 17 h / 0 - 5 °C 7: 5 percent / BBr3 / CH2Cl2 / 2 h / -70 °C View Scheme
参考文献
Terada; Tanoue; Hatada; Sakamoto
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 205 - 213
88818-38-6
→
反应条件
88818-28-4
1,4,5,8-四甲氧基萘-2-甲醛
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating View Scheme
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
88818-38-6
→
反应条件
88818-30-8
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 95 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 52 percent / cerium(IV) ammonium nitrate / acetonitrile; H2O / 0.5 h / 10 - 20 °C View Scheme
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
88818-38-6
→
反应条件
88818-32-0
反应条件
1: 84 percent / CuI / dimethylformamide; methanol / 30 h / Heating 2: 99 percent / POCl3 / CHCl3 / 6 h / Heating 3: 96 percent / tetrahydrofuran / 3 h / Ambient temperature 4: 87 percent / p-toluenesulfonic acid monohydrate / acetone / 3 h / 0 - 5 °C 5: 86 percent / diethyl ether; tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Terada, Akira; Tanoue, Yasuhiro; Hatada, Akira; Sakamoto, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1983 , # 18 p. 987 - 988
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