1-叔丁氧羰基-1,8-二氨基辛烷合成路线 (共 9 条)
反应条件
in chloroform T=20°C;
参考文献
Cinelli, Maris A.; Cordero, Brenda; Dexheimer, Thomas S.; Pommier, Yves; Cushman, Mark
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 20 p. 7145 - 7155
反应条件
ammonium hydroxide in methanol 48 h; Heating;
参考文献
Fixon-Owoo, Solomon; Levasseur, Frederic; Williams, Keith; Sabado, Thomas N.; Lowe, Mike; Klose, Markus; Mercier, A. Joffre; Fields, Paul; Atkinson, Jeffrey
Phytochemistry, 2003 , vol. 63, # 3 p. 315 - 334
参考文献
Tang, Wei; Fang, Shiyue
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 6003 - 6006
反应条件
1: 94 percent / methanol / -78 - 20 °C 2: 99 percent / tetrahydrofuran / 20 °C 3: 99 percent / aq. NH4OH / methanol / 48 h / Heating View Scheme
参考文献
Phytochemistry, , vol. 63, # 3 p. 315 - 334
反应条件
1: dimethylsulfoxide; diethyl ether / 2 h / Ambient temperature 2: aq. NaOH View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 26, # 10 p. 1510 - 1514
反应条件
1: 99 percent / tetrahydrofuran / 20 °C 2: 99 percent / aq. NH4OH / methanol / 48 h / Heating View Scheme
参考文献
Phytochemistry, , vol. 63, # 3 p. 315 - 334
反应条件
in diethyl ether; dimethyl sulfoxide 1 h; Ambient temperature;
参考文献
Hansen, J. B.; Nielsen, M. C.; Ehrbar, U.; Buchardt, O.
Synthesis, 1982 , # 5 p. 404 - 405
参考文献
Journal of Medicinal Chemistry, , vol. 26, # 10 p. 1510 - 1514
反应条件
in chloroform T=20°C;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 9 p. 4457 - 4478