in neat (no solvent) (Ar); std. Schlenk technique; mixt. of B compd. and Ph4Sn was stirred atambient temp. for 2 h; heated at 80°C overnight; distd. (100-115°C/0.10 Torr);
参考文献
Ly, Hanh V.; Forster, Taryn D.; Corrente, Andrea M.; Eisler, Dana J.; Konu, Jari; Parvez, Masood; Roesler, Roland
Organometallics, 2007 , vol. 26, # 7 p. 1750 - 1756
in neat (no solvent) inert gas; addn. of the Et4Sn at 0 ° C; stirring for 30 min at 40 ° C; addn. of pentane;; crystn. upon cooling to -75 ° C; removal of ClSn(C2H5)3; distillation of the borylethane at 55 ° C/E-3 Torr;;
