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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88888-30-6
合成路线
（共 16 条）
88888-30-6
→
反应条件
84010-89-9
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation 5: 40 percent / tetrahydrofuran View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
88888-22-6
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 1.) thionyl chloride, 2.) NH3 / 2.) ether, 0 deg C, 20-30 min View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
88888-24-8
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 75 percent / borane-methyl sulfide View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
88888-25-9
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation 5: 38 percent / 96 h / Irradiation 6: 64 percent / conc. nitric acid / acetic anhydride View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
88888-26-0
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation 5: 38 percent / 96 h / Irradiation 6: 64 percent / conc. nitric acid / acetic anhydride 7: 57 percent / H2 / 5percent Pd/C / ethanol / 2585.7 Torr View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
88888-32-8
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 75 percent / borane-methyl sulfide 5: 90 percent View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
84553-38-8
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 1.) thionyl chloride, 2.) NH3 / 2.) ether, 0 deg C, 20-30 min 5: 68 percent / trifluoroacetic anhydride, pyridine / dioxane / 10 °C View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
84553-40-2
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
84553-43-5
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation 5: iodine monochloride / CCl3F / Ambient temperature View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
88888-30-6
→
反应条件
84553-45-7
反应条件
1: 100 percent / diethyl ether 2: 85 percent / sulfur tetrafluoride 3: 90 percent / potassium hydroxide / H2O; ethanol 4: 72 percent / tert-butyl hypoiodite / Irradiation View Scheme
参考文献
Adcock, William; Abeywickrema, Anil N.; Kok, Gaik B.
Journal of Organic Chemistry, 1984 , vol. 49, p. 1387 - 1397
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