1: in tetrahydrofuran; toluene
T=20°C; 0.5 h; Inert atmosphere;
2: With n-hexyl lithium in tetrahydrofuran; hexane; toluene
T=-78 - -20°C;
参考文献
Magnus, Nicholas A.; Anzeveno, Peter B.; Coffey, D. Scott; Hay, David A.; Laurila, Michael E.; Schkeryantz, Jeffrey M.; Shaw, Bruce W.; Staszak, Michael A.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 560 - 567
1.1: dichloromethane / 0.08 h / 22.2 °C / |Inert atmosphere
1.2: 0.08 h / |Inert atmosphere
1.3: 2.5 h / 25 °C / |Inert atmosphere
2.1: tetrahydrofuran; toluene / 0.5 h / 20 °C / |Inert atmosphere
2.2: -78 - -20 °C
View Scheme
参考文献
Magnus, Nicholas A.; Anzeveno, Peter B.; Coffey, D. Scott; Hay, David A.; Laurila, Michael E.; Schkeryantz, Jeffrey M.; Shaw, Bruce W.; Staszak, Michael A.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 560 - 567
1.1: dichloromethane / 0.08 h / 22.2 °C / |Inert atmosphere
1.2: 0.08 h / |Inert atmosphere
1.3: 2.5 h / 25 °C / |Inert atmosphere
2.1: tetrahydrofuran; toluene / 0.5 h / 20 °C / |Inert atmosphere
2.2: -78 - -20 °C
View Scheme
参考文献
Magnus, Nicholas A.; Anzeveno, Peter B.; Coffey, D. Scott; Hay, David A.; Laurila, Michael E.; Schkeryantz, Jeffrey M.; Shaw, Bruce W.; Staszak, Michael A.
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 560 - 567
