Boc-1-氨基环丙基甲酸合成路线 （共 20 条）
反应条件
tetreamethyl ammonium hydroxide in acetonitrile 72 h; Ambient temperature;
参考文献
Khalil, Ehab M.; Subasinghe, Nalin L.; Johnson, Rodney L.
Tetrahedron Letters, 1996 , vol. 37, # 20 p. 3441 - 3444
反应条件
1: 94 percent / NaOH / 2-methyl-propan-2-ol; H2O / 1 h 2: 97 percent / H2 / 5percent Pd/C / methanol 3: 88 percent / KMnO4; NaOH / 2-methyl-propan-2-ol; H2O View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 11 p. 3965 - 3968
反应条件
sodium hydroxide; potassium permanganate in water; tert-butyl alcohol T=20°C; Oxidation;
参考文献
Pearson-Long, Morwenna S.M.; Beauseigneur, Alice; Karoyan, Philippe; Szymoniak, Jan; Bertus, Philippe
Synthesis, 2010 , # 20 art. no. T13410SS, p. 3410 - 3414
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 1.5 h; Ambient temperature;
参考文献
Kienzler, Thomas; Strazewski, Peter; Tamm, Christoph
Helvetica Chimica Acta, 1992 , vol. 75, # 4 p. 1078 - 1084
反应条件
1: 1-amino cyclopropane carboxylic acid hydrochloride With sodium hydroxide in 1,4-dioxane; water 0.166667 h; Cooling with ice; 2: di-tert-butyl dicarbonate in 1,4-dioxane; water T=20°C; 3 h;
参考文献
Salikov, Rinat F.; Platonov, Dmitry N.; Frumkin, Aleksandr E.; Lipilin, Dmitry L.; Tomilov, Yury V.
Tetrahedron, 2013 , vol. 69, # 16 p. 3495 - 3505
反应条件
triethylamine in 1,4-dioxane; water 2 h; Ambient temperature;
参考文献
Vaidyanathan, Ganesan; Wilson, Joseph W.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1815 - 1820
反应条件
methanol; sodium hydroxide T=25°C;
参考文献
Suzuki, M.; Gooch, E. E.; Stammer, C. H.
Tetrahedron Letters, 1983 , vol. 24, # 36 p. 3839 - 3840
反应条件
sodium hydroxide in ethanol; water 72 h; Ambient temperature;
参考文献
Wheeler, Thomas N.; Ray, John A.
Synthetic Communications, 1988 , vol. 18, # 2 p. 141 - 150
反应条件
1: 97 percent / H2 / 5percent Pd/C / methanol 2: 88 percent / KMnO4; NaOH / 2-methyl-propan-2-ol; H2O View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 11 p. 3965 - 3968
反应条件
triethylamine in 1,4-dioxane; water Ambient temperature;
参考文献
Husbands; Suckling
Tetrahedron, 1994 , vol. 50, # 32 p. 9729 - 9742
