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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88952-74-3
合成路线
（共 9 条）
88952-37-8
→
反应条件
88952-74-3
反应条件
bis(trichloromethyl) carbonate; N,N-dimethyl-formamide in 1,2-dichloro-ethane T=0 - 20°C; 2.5 h;
参考文献
Su; Zhu; Li
Organic Preparations and Procedures International, 2009 , vol. 41, # 1 p. 69 - 75
6627-55-0
2-溴-4-甲基苯酚
+
201230-82-2
+
766-97-2
4-甲苯基乙炔
→
反应条件
88952-74-3
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1-methyl-2-((4-phenyl-1H-1,2,3-triazol-1-yl)methyl)-1H-benzo[d]imidazole; n-dipropylamine T=130°C; P=15001.5 Torr; 24 h; Autoclave;
参考文献
Liu, Jianming; Liu, Muwen; Yue, Yuanyuan; Zhang, Ningfei; Zhang, Yuanli; Zhuo, Kelei
Tetrahedron Letters, 2013 , vol. 54, # 14 p. 1802 - 1807
6627-55-0
2-溴-4-甲基苯酚
+
201230-82-2
+
766-97-2
4-甲苯基乙炔
→
反应条件
61976-50-9
+
88952-74-3
反应条件
bis-triphenylphosphine-palladium(II) chloride; 1-methyl-2-((4-phenyl-1H-1,2,3-triazol-1-yl)methyl)-1H-benzo[d]imidazole; n-dipropylamine; diisopropylamine T=130°C; P=15001.5 Torr; 24 h; Autoclave; regioselective reaction;
参考文献
Liu, Jianming; Liu, Muwen; Yue, Yuanyuan; Zhang, Ningfei; Zhang, Yuanli; Zhuo, Kelei
Tetrahedron Letters, 2013 , vol. 54, # 14 p. 1802 - 1807
4010-25-7
→
反应条件
88952-74-3
反应条件
potassium carbonate in N,N-dimethyl-formamide 0.166667 h; Heating;
参考文献
Wurm, Gotthard; Nordmann, Matthias
Archiv der Pharmazie (Weinheim, Germany), 1988 , vol. 321, p. 555 - 558
1450-72-2
2-羟基-5-甲基苯乙酮
→
反应条件
88952-74-3
反应条件
1: 82 percent / pyridine / 0.5 h / 50 °C 2: 96 percent / pyridine; KOH / 1.5 h / 50 °C 3: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
106-44-5
对甲酚
→
反应条件
88952-74-3
反应条件
1: pyridine 2: AlCl3 3: 82 percent / pyridine / 0.5 h / 50 °C 4: 96 percent / pyridine; KOH / 1.5 h / 50 °C 5: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
88952-74-3
反应条件
1: AlCl3 2: 82 percent / pyridine / 0.5 h / 50 °C 3: 96 percent / pyridine; KOH / 1.5 h / 50 °C 4: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
874-60-2
对甲基苯甲酰氯
→
反应条件
88952-74-3
反应条件
1: 82 percent / pyridine / 0.5 h / 50 °C 2: 96 percent / pyridine; KOH / 1.5 h / 50 °C 3: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
99-94-5
对甲基苯甲酸
→
反应条件
88952-74-3
反应条件
1: SOCl2; DMF / 2.5 h / Heating 2: 82 percent / pyridine / 0.5 h / 50 °C 3: 96 percent / pyridine; KOH / 1.5 h / 50 °C 4: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
