1,4-二甲氧基-2-硝基苯合成路线 （共 38 条）
反应条件
nitrogen(IV) oxide in dichloromethane in the dark; -78 deg C, 2 min; RT, 15 min;
参考文献
Hajipour, Abdol R.; Ruoho, Arnold E.
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 2 p. 221 - 226
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide T=140°C; P=760.051 Torr; 36 h;
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 10 p. 2959 - 2962
Angew. Chem., 2013 , vol. 125, # 10 p. 3031 - 3035,4
反应条件
Oxonereg;; potassium hydroxide; disodium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water; acetone T=0°C; pH=7.5-8.5, excess of OXONE (8 eq);
参考文献
Zabrowsky, Daniel L.; Moormann, Alan E.; Beck, Kenneth R.
Tetrahedron Letters, 1988 , vol. 29, # 36 p. 4501 - 4504
反应条件
sodium nitrate; silver nitrate; potassium nitrate; potassium hexacyanoferrate(III) T=160°C; 6 h;
参考文献
Journal of Organic Chemistry, , vol. 73, # 16 p. 6148 - 6151
反应条件
Oxonereg;; potassium hydroxide; disodium hydrogenphosphate; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water; acetone T=0°C; pH=7.5-8.5; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 29, # 36 p. 4501 - 4504
反应条件
TNM in acetonitrile T=20°C; 4 h; Irradiation;
参考文献
Acta Chemica Scandinavica, , vol. 51, # 6-7 p. 718 - 732
反应条件
sulfuric acid; nitric acid; acetic acid T=25°C; Nitration; oxidative demethylation; 24 h;
参考文献
Journal of Chemical Research - Part S, , # 3 p. 106 - 107
反应条件
nitric acid; silica gel in dichloromethane 0.0833333 h; Ambient temperature; Product distribution;
参考文献
Synthetic Communications, , vol. 16, # 6 p. 681 - 688
反应条件
1: potassium tert-butylate / ethanol / 1 h 2: copper diacetate; silver carbonate; oxygen / N,N-dimethyl-formamide / 36 h / 140 °C / 760.05 Torr View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 10 p. 2959 - 2962
Angew. Chem., , vol. 125, # 10 p. 3031 - 3035,4
反应条件
nitric acid T=65 - 68°C;
参考文献
Anilinokr. Promysl., , vol. 4, p. 7,9, 10
Chem. Zentralbl., , vol. 105, # II p. 1617
