4-甲基-2-硝基苯胺合成路线 （共 173 条）
反应条件
1.1: H2SO4; NaNO2 1.2: 51.8 percent / Cu2Br2 2.1: 84.9 percent / Fe; CH3COOH 3.1: HCl; NaBF4; NaNO2 3.2: 57.7 percent / Heating 4.1: 34.9 percent / C2H5Br; Mg / tetrahydrofuran View Scheme
参考文献
Zou, Xinzhuo; Qiu, Zongxing
Journal of Fluorine Chemistry, 2002 , vol. 116, # 2 p. 173 - 179
反应条件
1: 22.3 g / glacial acetic acid / 0.5 h / Heating 2: H2 / 10percent Pd on charcoal / ethanol / 6 h / 2280 Torr View Scheme
参考文献
Cheeseman, G. W. H.; Hawi, A. A.; Varvounis, G.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 423 - 427
反应条件
1: 60 percent 2: 65 percent / 1 M NaOH / pyridine / 1 h 3: sodium dithionite / ethanol; H2O View Scheme
参考文献
Ahmed, Yusuf; Qureshi, M. Ikram; Habib, M. Saleem; Farooqi, M. Amir
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 3 p. 1145 - 1148
反应条件
1: With sulfuric acid; sodium nitrite 2: With copper(I) bromide
参考文献
Zou, Xinzhuo; Qiu, Zongxing
Journal of Fluorine Chemistry, 2002 , vol. 116, # 2 p. 173 - 179
反应条件
1: aqueous H2SO4 / Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuBr 2: tin (II)-chloride; aqueous hydrochloric acid; diethyl ether View Scheme
参考文献
Zou, Xinzhuo; Qiu, Zongxing
Journal of Fluorine Chemistry, 2002 , vol. 116, # 2 p. 173 - 179
反应条件
acetic acid 0.5 h; Heating;
参考文献
Cheeseman, G. W. H.; Hawi, A. A.; Varvounis, G.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 423 - 427
反应条件
1: Raney Ni, H2 / ethanol 2: ethanol View Scheme
参考文献
Cavagnol; Wiselogle
Journal of the American Chemical Society, 1947 , vol. 69, p. 795,796
反应条件
2: tin; hydrochloric acid View Scheme
参考文献
Niementowski
Chemische Berichte, 1899 , vol. 32, p. 1477
反应条件
durch Entamidierung;
参考文献
Beilstein; Kuhlberg
Justus Liebigs Annalen der Chemie, 1870 , vol. 155, p. 13
反应条件
1: Diazotization.Erwaermen der Diazoniumsulfatloesung mit KI auf dem Wasserbade 2: alcohol; iron monoxide hydrate View Scheme
参考文献
Chemische Berichte, , vol. 39, p. 269
