4-甲基-2-硝基苯胺合成路线 （共 173 条）
反应条件
dipotassium peroxodisulfate; sulfuric acid
24 h;
参考文献
Dobrodei; El'tsov
Russian Journal of General Chemistry, 1998 , vol. 68, # 4 p. 620 - 629
参考文献
Bamberger; Huebner
Chemische Berichte, 1903 , vol. 36, p. 3826
反应条件
1: 98 percent / Br2; AcOH / 0.5 h
2: 83 percent / SnCl2*H2O; aq. HCl / ethanol / 4 h / 60 °C
View Scheme
参考文献
Yasui, Yoshizumi; Frantz, Derik K.; Siegel, Jay S.
Organic Letters, 2006 , vol. 8, # 22 p. 4989 - 4992
反应条件
1: 1-amino-2-nitro-4-methylbenzene With sulfuric acid; sodium nitrite
T=10 - 15°C; 0.833333 h;
2: sodium isothiocyanate With ammonium sulfate; Fe2(S04)3 in water
T=12°C; 14 h;
参考文献
Matveev; Ponyaev; El'tsov
Russian Journal of General Chemistry, 2001 , vol. 71, # 8 p. 1286 - 1292
反应条件
in N,N-dimethyl-formamide
Cooling with ice;
参考文献
Yarovenko; Polushina; Levchenko; Zavarzin; Krayushkin; Kotovskaya; Charushin
Russian Chemical Bulletin, 2009 , vol. 58, # 6 p. 1276 - 1280
参考文献
Platt
Journal of the Chemical Society, 1948 , p. 1310,1312
参考文献
Platt
Journal of the Chemical Society, 1948 , p. 1310,1312
反应条件
1: aqueous H2SO4 / Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuBr
2: tin; aqueous hydrochloric acid; graphite
3: Diazotization
4: diethyl ether / anschliessend Behandeln mit Eis und wss. HCl
View Scheme
参考文献
Borsche; Scriba
Justus Liebigs Annalen der Chemie, 1939 , vol. 541, p. 283,290
反应条件
1: potassium carbonate; copper / 160 °C
2: acetic acid; zinc
3: FeCl3; aqueous HCl
View Scheme
参考文献
Tomlinson
Journal of the Chemical Society, 1939 , p. 158,161
反应条件
copper; potassium carbonate
T=160°C;
参考文献
Tomlinson
Journal of the Chemical Society, 1939 , p. 158,161
