4-甲基-2-硝基苯胺合成路线 （共 173 条）
反应条件
1: Raney Ni, H2 / ethanol 2: ethanol 3: 11 percent / H2SO4, air / H2O / 9 h / Irradiation View Scheme
参考文献
El'tsov; Selitrenikov; Rtishchev
Russian Journal of General Chemistry, 1997 , vol. 67, # 2 p. 285 - 294
反应条件
Diazotization.Behandlung des Diazoniumperbromids mit Ammoniak;
参考文献
Monge, Antonio; Palop, Juan A.; Cerain, Adela Lopez de; Senador, Virginia; Martinez-Crespo, Francisko J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 10 p. 1786 - 1792
反应条件
1: With sodium tris(acetoxy)borohydride; acetic acid in dichloromethane T=20°C; 1 h; 2: With sodium hydrogencarbonate in water; ethyl acetate
参考文献
Boyce, Rustum S.; Guo, Hongyan; Mendenhall, Kris G.; Walter, Annette O.; Wang, Weibo; Xia, Yia
Patent: US2006/84687 A1, 2006 ;
Location in patent: Page/Page column 21 ;
反应条件
in water T=100°C; 1.5 h;
参考文献
Kommi, Damodara N.; Kumar, Dinesh; Bansal, Rohit; Chebolu, Rajesh; Chakraborti, Asit K.
Green Chemistry, 2012 , vol. 14, # 12 p. 3329 - 3335
反应条件
1: sat. NaHCO3 / CH2Cl2 / Ambient temperature 2: 80 percent / benzyltriethylammonium chloride, aq. NaOH / toluene / Ambient temperature View Scheme
参考文献
Brown, Samuel A.; Rizzo, Carmelo J.
Synthetic Communications, 1996 , vol. 26, # 21 p. 4065 - 4080
参考文献
Rao; Ratnam
Proceedings - Indian Academy of Sciences, Section A, 1956 , vol. 44, p. 331,336
反应条件
1: man ersetzt die NH2-Gruppe durch Chlor, reduziert mit Zinn und Salzsaeure und ersetzt die neugebildete NH2-Gruppe durch Brom 2: HNO3 3: PCl5 / 130 - 140 °C View Scheme
参考文献
Cohen; Raper
Journal of the Chemical Society, 1904 , vol. 85, p. 1269
参考文献
Siqueira, Fernanda A.; Taylor, Jason G.; Correia, Carlos Roque D.
Tetrahedron Letters, 2010 , vol. 51, # 16 p. 2102 - 2105
反应条件
1: HCl / 100 °C 2: aq. NaOH / 1 h / 100 °C 3: 25 percent / 30percent aq. H2O2; HOAc / 4 h / 50 °C View Scheme
参考文献
Hay, Michael P.; Gamage, Swarna A.; Kovacs, Mary S.; Pruijn, Frederik B.; Anderson, Robert F.; Patterson, Adam V.; Wilson, William R.; Brown, J. Martin; Denny, William A.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 1 p. 169 - 182
反应条件
hydrogenchloride; sodium acetate; sodium nitrite 1) 0 deg C, 2) water; Multistep reaction;
参考文献
Jain; Pandey
Journal of the Indian Chemical Society, 1989 , vol. 66, # 5 p. 350 - 352
