1,3-二甲基-4-硝基苯合成路线 (共 60 条)
反应条件
Bi(NO3)3; sulfuric acid; silica gel T=25°C; 0.0666667 h;
参考文献
Hajipour; Zarei; Ruoho
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 10 p. 1493 - 1495
反应条件
tert.-butylhydroperoxide; potassium iodide in water; acetonitrile T=80°C; 15 h;
参考文献
Reddy, K. Rajender; Maheswari, C. Uma; Venkateshwar; Kantam, M. Lakshmi
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 1-2 p. 93 - 96
反应条件
lanthanium(III) nosylate; nitric acid in 1,2-dichloro-ethane 16 h; Heating; Product distribution;
参考文献
Tetrahedron Letters, , vol. 45, # 15 p. 3137 - 3139
反应条件
trifluorormethanesulfonic acid T=100°C;
参考文献
Barrow, Peter; Bullen, John V.; Dent, Andrea; Murphy, Timothy; Ridd, John H.; Sabek, Omaima
Journal of the Chemical Society, Chemical Communications, 1986 , # 22 p. 1649 - 1650
反应条件
nitric acid; ytterbium(III) pefluorooctanesulfonate; lithium perchlorate; β-MoO3 T=60°C; 48 h; Title compound not separated from byproducts.;
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 12 p. 1329 - 1333
反应条件
dinitrogen tetraoxide in dichloromethane T=25°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 12 p. 3314 - 3325
反应条件
nitrogen(IV) oxide; ozone in dichloromethane T=-10°C; 3 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 14 p. 1591 - 1598
反应条件
trifluorormethanesulfonic acid T=110°C;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 10 p. 1681 - 1685
反应条件
1: dimethylformamide / 20 °C 2: 80 percent / MgCl2*6H2O / N,N-dimethyl-acetamide / 12 h / 140 - 150 °C View Scheme
参考文献
Synthesis, , # 12 p. 1659 - 1661
反应条件
in benzene 24 h; Heating;
参考文献
Jung, Michael E.; Grove, David D.
Journal of the Chemical Society, Chemical Communications, 1987 , p. 753 - 755