1,3-二甲基-4-硝基苯合成路线 （共 60 条）
反应条件
antimony(V) pentachloride; chlorine
参考文献
I. G. Farbenind.
Patent: DE510438 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 447
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Gen. Aniline Works
Patent: US1762018 , 1927 ;
反应条件
sulfuric acid; chlorine; iron(III) chloride
参考文献
I. G. Farbenind.
Patent: DE510438 , 1926 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 447
Full Text Show Details
Gen. Aniline Works
Patent: US1762018 , 1927 ;
反应条件
1: durch Reduktion
2: diluted sulfuric acid
View Scheme
参考文献
Bamberger; Brady
Chemische Berichte, 1900 , vol. 33, p. 3651
参考文献
Bamberger
Chemische Berichte, 1926 , vol. 59, p. 423
反应条件
nitric acid
T=20°C; 1 h;
参考文献
Havlik, Martin; Kral, Vladimir; Dolensky, Bohumil
Organic Letters, 2006 , vol. 8, # 21 p. 4867 - 4870
反应条件
1: diluted alcohol; zinc dust; ammonium chloride
2: potassium dichromate; sulfuric acid
View Scheme
参考文献
v. Pechmann; Nold
Chemische Berichte, 1898 , vol. 31, p. 559
反应条件
1: permanganate
2: concentrated sulfuric acid
4: tin; concentrated hydrochloric acid
View Scheme
参考文献
Axer
Monatshefte fuer Chemie, 1920 , vol. 41, p. 155
反应条件
1: 55 percent / KMnO4 / H2O / 2 h / Heating
2: 56 percent / p-toluenesulfonamide, PCl5 / 0.5 h / 200 - 205 °C
View Scheme
参考文献
Kornblum, Nathan; Fifolt, Michael J.
Tetrahedron, 1989 , vol. 45, # 5 p. 1311 - 1322
反应条件
sulfuric acid; nitric acid in water
1 h;
参考文献
Zhang, Aimin; Han, Yaohua; Yamato, Kazuhiro; Zeng, Xiao Cheng; Gong, Bing
Organic Letters, 2006 , vol. 8, # 5 p. 803 - 806
反应条件
nitric acid
T=20°C; 1 h;
参考文献
Havlik, Martin; Kral, Vladimir; Dolensky, Bohumil
Organic Letters, 2006 , vol. 8, # 21 p. 4867 - 4870
