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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-氯苯甲醛
合成路线
（共 849 条）
100-71-0
2-乙基吡啶
+
89-98-5
2-氯苯甲醛
→
反应条件
6772-82-3
反应条件
acetic anhydride Heating;
参考文献
Arai, Sadao; Arai, Hitoshi; Tabuchi, Kunihisa; Yamagishi, Takamichi; Hida, Mitsuhiko
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 1 p. 215 - 220
6066-82-6
N-羟基丁二酰亚胺
+
89-98-5
2-氯苯甲醛
→
反应条件
68388-08-9
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in ethyl acetate T=20 - 70°C; 12 h;
参考文献
Tan, Bin; Toda, Narihiro; Barbas III, Carlos F.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12538 - 12541
Angew. Chem., 2012 , vol. 124, # 50 p. 12706 - 12709,4
89-98-5
2-氯苯甲醛
→
反应条件
807343-03-9
N-(2-氯苄基)-1-丙胺
反应条件
1: Na2SO4 / CH2Cl2 / 2 h 2: 1.77 g / NaBH4 / methanol / 1 h / 20 °C View Scheme
参考文献
Orito, Kazuhiko; Horibata, Akiyoshi; Nakamura, Takatoshi; Ushito, Harumi; Nagasaki, Hideo; Yuguchi, Motoki; Yamashita, Satoshi; Tokuda, Masao
Journal of the American Chemical Society, 2004 , vol. 126, # 44 p. 14342 - 14343
89-98-5
2-氯苯甲醛
→
反应条件
82238-29-7
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: acetonitrile / 3 h / Ambient temperature 6: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
89-98-5
2-氯苯甲醛
→
反应条件
82238-30-0
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 99.6 percent / diethyl ether / 1 h / Heating 3: 69.2 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: toluene / 6 h / Heating; thermal or base catalysed rearrangement View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
57597-62-3
+
89-98-5
2-氯苯甲醛
→
反应条件
825638-07-1
反应条件
暂无反应条件数据
参考文献
Goehring, Wolfgang; Harrington, Peter John; Hodges, Lewis M.; Johnston, David A.; Rimmler, Goesta
Patent: US2005/14792 A1, 2005 ;
Location in patent: Page/Page column 8 ;
US 20050014792 A1
141-32-2
+
89-98-5
2-氯苯甲醛
→
反应条件
826991-00-8
反应条件
tetrabutylammomium bromide; potassium carbonate in N,N-dimethyl-formamide T=100°C; Mizoroki-Heck cross-coupling reaction; 24 h;
参考文献
Tamami, Bahman; Ghasemi, Soheila
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 322, # 1-2 p. 98 - 105
89-98-5
2-氯苯甲醛
+
1611-78-5
→
反应条件
82700-44-5
反应条件
perchloric acid in acetic anhydride 48 h; Ambient temperature;
参考文献
Arnold, Z.; Kral, V.; Dvorak, D.
Tetrahedron Letters, 1982 , vol. 23, # 16 p. 1725 - 1726
89-98-5
2-氯苯甲醛
→
反应条件
828-81-9
反应条件
1: sodium acetate / water / 20 °C 2: anhydrous iron chloride; sodium acetate / acetic acid / 0.5 h / 20 °C View Scheme
参考文献
Rajak, Harish; Agarawal, Avantika; Parmar, Poonam; Thakur, Bhupendra Singh; Veerasamy, Ravichandran; Sharma, Prabodh Chander; Kharya, Murli Dhar
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 19 p. 5735 - 5738
89-98-5
2-氯苯甲醛
→
反应条件
832724-77-3
反应条件
1: 99 percent / magnesium sulfate / CH2Cl2 / 1 h / Heating 2: 100 percent / bromine / CH2Cl2 / 0.5 h / 20 °C 3: 95 percent / sodium borohydride / methanol / 1 h / Heating View Scheme
参考文献
D'hooghe, Matthias; Waterinckx, Alex; De Kimpe, Norbert
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 227 - 232
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