(1H-吲哚-3-基)-对甲苯-甲酮合成路线 （共 7 条）
反应条件
titanium tetrachloride in dichloromethane
T=25°C; 2 h;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.; He, Hai-Ying
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5720 - 5723
反应条件
[2,2']bipyridinyl; (1S)-10-camphorsulfonic acid; water; palladium diacetate
T=120°C; 36 h; ConcentrationReagent/catalystSolvent;
参考文献
Jiang, Tao-Shan; Wang, Guan-Wu
Organic Letters, 2013 , vol. 15, # 4 p. 788 - 791
反应条件
aluminum oxide in neat (no solvent)
T=100°C; 0.116667 h; Microwave irradiationGreen chemistry; regioselective reaction;
参考文献
Lai, Qiu Yu; Liao, Rong Su; Wu, Shao Yong; Zhang, Jia Xin; Duan, Xin Hong
New Journal of Chemistry, 2013 , vol. 37, # 12 p. 4069 - 4076
反应条件
tert.-butylhydroperoxide; 2-oxo-3,3-dimethyl-butanoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; iron(II) chloride in decane; dimethyl sulfoxide
T=25°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Wu, Wenliang; Su, Weiping
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 11924 - 11927
反应条件
trichlorophosphate
T=0 - 83°C; Vilsmeier-Haack Formylation; 2.5 h;
参考文献
Paul, Nidhin; Muthusubramanian, Shanmugam
Helvetica Chimica Acta, 2013 , vol. 96, # 3 p. 452 - 457
参考文献
Dainippon Sumitomo Pharma Co., Ltd.
Patent: EP1837329 A1, 2007 ;
反应条件
1: 91 percent / Et3N / tetrahydrofuran / Heating
2: 92 percent / TiCl4 / CH2Cl2 / 2 h / 25 °C
View Scheme
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.; He, Hai-Ying
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5720 - 5723
