反应条件
1: TsCl / CCl4; pyridine / 15 h / 4 °C
2: 1.) NaN3, sulphuric acid; 2.) HCl (4M) / 1.) ether, reflux, 30 h; 2.) 6 h
View Scheme
参考文献
Casey, Michael; Moody, Christopher; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1389 - 1394