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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89006-89-3
合成路线
（共 5 条）
89006-88-2
→
反应条件
89006-89-3
反应条件
trichlorophosphate in N,N-dimethyl-formamide 0 deg C then rt.;
参考文献
Seki; Moriya; Matsumoto; Takashima; Mori; Odawara; Takeyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 11 p. 4435 - 4440
89007-04-5
→
反应条件
89006-89-3
反应条件
1: 70 percent / sodium bicarbonate / ethyl acetate; H2O / Ambient temperature 2: 56 percent / 61 percent sodium hydride in paraffine / dimethylformamide / -50 deg C, up to 10 deg C 3: 84 percent / phosphoryl chloride / dimethylformamide / 0 deg C then rt. View Scheme
参考文献
Seki; Moriya; Matsumoto; Takashima; Mori; Odawara; Takeyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 11 p. 4435 - 4440
122-01-0
氯化对氯苯甲酰
→
反应条件
89006-89-3
反应条件
1: 70 percent / sodium bicarbonate / ethyl acetate; H2O / Ambient temperature 2: 56 percent / 61 percent sodium hydride in paraffine / dimethylformamide / -50 deg C, up to 10 deg C 3: 84 percent / phosphoryl chloride / dimethylformamide / 0 deg C then rt. View Scheme
参考文献
Seki; Moriya; Matsumoto; Takashima; Mori; Odawara; Takeyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 11 p. 4435 - 4440
89007-05-6
→
反应条件
89006-89-3
反应条件
1: 56 percent / 61 percent sodium hydride in paraffine / dimethylformamide / -50 deg C, up to 10 deg C 2: 84 percent / phosphoryl chloride / dimethylformamide / 0 deg C then rt. View Scheme
参考文献
Seki; Moriya; Matsumoto; Takashima; Mori; Odawara; Takeyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 11 p. 4435 - 4440
89006-89-3
→
反应条件
89006-95-1
反应条件
potassium hydroxide in methanol; water Ambient temperature;
参考文献
Seki; Moriya; Matsumoto; Takashima; Mori; Odawara; Takeyama
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 11 p. 4435 - 4440
