2-溴-3’-甲氧基苯甲酮合成路线 (共 8 条)
反应条件
in acetonitrile 36 h; Irradiation;
参考文献
Journal of Organic Chemistry, , vol. 72, # 25 p. 9786 - 9789
反应条件
in acetonitrile 36 h; Irradiation;
参考文献
Moorthy, Jarugu Narasimha; Samanta, Subhas
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9786 - 9789
反应条件
4 A molecular sieve; pyridinium chlorochromate in dichloromethane
T=20°C; 2 h;
参考文献
Moorthy, Jarugu Narasimha; Samanta, Subhas
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9786 - 9789
反应条件
C57H43IP2Pd; potassium carbonate in 1,4-dioxane
T=90°C; carbonylative Suzuki coupling; P=3750.38 Torr; 12 h; Autoclave;
参考文献
Kaganovsky, Luba; Gelman, Dmitri; Rueck-Braun, Karola
Journal of Organometallic Chemistry, 2010 , vol. 695, # 2 p. 260 - 266
反应条件
1.1: magnesium / tetrahydrofuran / 1 h / Reflux
1.2: 0 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 15 h / 20 °C
View Scheme
参考文献
Sui, Yao-Zong; Zhang, Xi-Chang; Wu, Jun-Wen; Li, Shijun; Zhou, Ji-Ning; Li, Min; Fang, Wenjun; Chan, Albert S. C.; Wu, Jing
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7486 - 7492
反应条件
1.1: magnesium / tetrahydrofuran / 1 h / Reflux
1.2: 0 °C / Inert atmosphere
2.1: pyridinium chlorochromate / dichloromethane / 15 h / 20 °C
View Scheme
参考文献
Sui, Yao-Zong; Zhang, Xi-Chang; Wu, Jun-Wen; Li, Shijun; Zhou, Ji-Ning; Li, Min; Fang, Wenjun; Chan, Albert S. C.; Wu, Jing
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7486 - 7492
反应条件
1: diethyl ether / 3 h / 0 - 20 °C / |Inert atmosphere
2: pyridinium chlorochromate; silica gel / dichloromethane / 2 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Mahendar, Lodi; Satyanarayana, Gedu
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2059 - 2074
反应条件
in acetonitrile
36 h; Irradiation;
参考文献
Moorthy, Jarugu Narasimha; Samanta, Subhas
Journal of Organic Chemistry, 2007 , vol. 72, # 25 p. 9786 - 9789