N-乙酰基-2’-C-甲基鸟苷-2’,3’,5’-三苯甲酸酯合成路线 （共 4 条）
参考文献
McGuigan, Christopher; Perrone, Plinio; Madela, Karolina; Neyts, Johan
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 15 p. 4316 - 4320
反应条件
1: 2-N-Acetylguanine With pyridine; 1,1,1,3,3,3-hexamethyl-disilazane
0.5 h; Heating;
2: 1,2,3,5-tetra-O-benzoyl-2-C-methyl-α,β-D-ribofuranose With trimethylsilyl trifluoromethanesulfonate in para-xylene
T=140°C; 6 h;
参考文献
Li, Nan-Sheng; Piccirilli, Joseoh A.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 4018 - 4020
反应条件
trimethylsilyl trifluoromethanesulfonate in toluene
T=111°C; 24 h; Title compound not separated from byproducts;
参考文献
Li, Nan-Sheng; Piccirilli, Joseoh A.
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 4018 - 4020
反应条件
trimethylsilyl trifluoromethanesulfonate; lithium hexamethyldisilazane in para-xylene
参考文献
McGuigan, Christopher; Perrone, Plinio; Madela, Karolina; Neyts, Johan
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 15 p. 4316 - 4320
