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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
89018-72-4
合成路线
（共 15 条）
105485-74-3
→
反应条件
89018-72-4
反应条件
ammonium formate; palladium on activated charcoal in methanol 1 h; Heating;
参考文献
xxx
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2000 , vol. 39, # 11 p. 817 - 821
86-81-7
3,4,5-三甲氧基苯甲醛
→
反应条件
89018-72-4
反应条件
1: 79 percent / n-Bu2NH / diethyl ether / 3 h / 20 °C 2: TsOH / benzene / 0.5 h / 50 °C 3: NaH / ethanol / 18 h / 20 °C 4: aq. HCl / methanol / 1 h / 20 °C 5: H2 / Pd/C / 2 h / 20 °C View Scheme
参考文献
Wu, Maojiang; Sun, Qiming; Yang, Chunhao; Chen, Dongdong; Ding, Jian; Chen, Yi; Lin, Liping; Xie, Yuyuan
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 4 p. 869 - 873
130190-35-1
→
反应条件
89018-72-4
反应条件
1: TsOH / benzene / 0.5 h / 50 °C 2: NaH / ethanol / 18 h / 20 °C 3: aq. HCl / methanol / 1 h / 20 °C 4: H2 / Pd/C / 2 h / 20 °C View Scheme
参考文献
Wu, Maojiang; Sun, Qiming; Yang, Chunhao; Chen, Dongdong; Ding, Jian; Chen, Yi; Lin, Liping; Xie, Yuyuan
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 4 p. 869 - 873
931407-28-2
→
反应条件
89018-72-4
反应条件
1: NaH / ethanol / 18 h / 20 °C 2: aq. HCl / methanol / 1 h / 20 °C 3: H2 / Pd/C / 2 h / 20 °C View Scheme
参考文献
Wu, Maojiang; Sun, Qiming; Yang, Chunhao; Chen, Dongdong; Ding, Jian; Chen, Yi; Lin, Liping; Xie, Yuyuan
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 4 p. 869 - 873
55667-12-4
2-苄氧基-4-溴甲基-1-甲氧基苯
→
反应条件
89018-72-4
反应条件
1: 50 percent / n-butyl lithium / tetrahydrofuran / 3 h / -30 °C 2: mercuric chloride / methanol; tetrahydrofuran / 24 h / 130 °C 3: trifluoroacetic acid / 3 h / Ambient temperature View Scheme
参考文献
Annapurna, G. S.; Deshpande, V. H.
Synthetic Communications, 1983 , vol. 13, # 13 p. 1075 - 1082
1136-86-3
3',4',5'-三甲氧基苯乙酮
→
反应条件
89018-72-4
反应条件
1: 85 percent / NaOH / methanol / 18 h / 25 - 30 °C 2: 80 percent / aq. NaOH; aq. H2O2 / methanol; acetone / 0.75 h / 20 - 25 °C 3: 87 percent / NaOH / H2O; ethanol / 4 h / Heating 4: 89 percent / NaIO4 / acetone; acetic acid; H2O / 7 h / 25 °C 5: 95 percent / HCOONH4 / Pd/C / methanol / 1 h / Heating View Scheme
参考文献
xxx
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2000 , vol. 39, # 11 p. 817 - 821
330468-38-7
→
反应条件
89018-72-4
反应条件
1: 87 percent / NaOH / H2O; ethanol / 4 h / Heating 2: 89 percent / NaIO4 / acetone; acetic acid; H2O / 7 h / 25 °C 3: 95 percent / HCOONH4 / Pd/C / methanol / 1 h / Heating View Scheme
参考文献
xxx
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2000 , vol. 39, # 11 p. 817 - 821
330468-40-1
→
反应条件
89018-72-4
反应条件
1: 89 percent / NaIO4 / acetone; acetic acid; H2O / 7 h / 25 °C 2: 95 percent / HCOONH4 / Pd/C / methanol / 1 h / Heating View Scheme
参考文献
xxx
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 2000 , vol. 39, # 11 p. 817 - 821
105485-73-2
→
反应条件
89018-72-4
反应条件
1: 1) NaH / 1) DMF, 1 h, 2) DMF, 24 h 2: 85 percent / H2 / 10percent Pd/C / ethanol / 2.5 h / 760 Torr / Ambient temperature View Scheme
参考文献
Latey, P. P.; Deshpande, V. H.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 299 - 300
621-59-0
3-羟基-4-甲氧基苯甲醛
→
反应条件
89018-72-4
反应条件
1: 80 percent / potassium carbonate / acetone / 5 h / Heating 2: 83 percent / sodium borohydride / ethanol / 0.5 h 3: 88 percent / PBr3 / benzene / 0.5 h / 5 °C 4: 50 percent / n-butyl lithium / tetrahydrofuran / 3 h / -30 °C 5: mercuric chloride / methanol; tetrahydrofuran / 24 h / 130 °C 6: trifluoroacetic acid / 3 h / Ambient temperature View Scheme
参考文献
Annapurna, G. S.; Deshpande, V. H.
Synthetic Communications, 1983 , vol. 13, # 13 p. 1075 - 1082
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