methanesulfonyl chloride in N,N-dimethyl-formamide
T=60 - 70°C; 3 h;
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
1: 93 percent / BF3*Et2O / 1 h / 60 - 70 °C
2: 91 percent / methanesulphonyl chloride / dimethylformamide / 3 h / 60 - 70 °C
View Scheme
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
1: 93 percent / BF3*Et2O / 1 h / 60 - 70 °C
2: 91 percent / methanesulphonyl chloride / dimethylformamide / 3 h / 60 - 70 °C
View Scheme
参考文献
Waehaelae, Kristiina; Hase, Tapio A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 3005 - 3008
