1: CH2Cl2 / 2 h / Ambient temperature
2: 57 percent / pyridine, bromine / CH2Cl2 / from -78 deg C to room temp.
3: 92 percent / diethyl ether / 30 h / from -78 deg C to room temp.
View Scheme
参考文献
Easton, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 153 - 158
1: 57 percent / pyridine, bromine / CH2Cl2 / from -78 deg C to room temp.
2: 92 percent / diethyl ether / 30 h / from -78 deg C to room temp.
View Scheme
参考文献
Easton, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 153 - 158
