2,3,4,6-四-O-苄基-α-D-吡喃葡萄糖酰氟合成路线 （共 25 条）
反应条件
silicon tetrafluoride in acetonitrile T=0°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Hashimoto, S.; Hayashi, M.; Noyori, R.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1379 - 1382
反应条件
1: 96 percent / BF3*Et2O; 4 Angstroem molecular sieves / CH2Cl2 / -78 - 20 °C 2: 84 percent / dioxane; aq. NaOH / 24 h / 20 °C 3: 84 percent / I2 / dimethylsulfoxide / 0.5 h / Heating 4: 100 percent / H2 / Pd-C / ethanol; ethyl acetate / 20 °C View Scheme
参考文献
Kumazawa; Kimura; Matsuba; Sato; Onodera
Carbohydrate Research, 2001 , vol. 334, # 3 p. 183 - 193
反应条件
silicon tetrafluoride in acetonitrile T=0°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Hashimoto, S.; Hayashi, M.; Noyori, R.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1379 - 1382
反应条件
silicon tetrafluoride in acetonitrile T=0°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Hashimoto, S.; Hayashi, M.; Noyori, R.
Tetrahedron Letters, 1984 , vol. 25, # 13 p. 1379 - 1382
反应条件
1: BF3*Et2O / 21 h / Ambient temperature 2: 86 percent / H2 / 10percent Pd/C / methanol / 24 h / 750.06 Torr / Ambient temperature View Scheme
参考文献
Thiem, Joachim; Kleeberg, Matthias; Klaska, Karl-Heinz
Carbohydrate Research, 1989 , vol. 189, p. 65 - 78
