1-(叔丁基二甲基硅基)-3-氯丙烷合成路线 (共 4 条)
反应条件
zinc tetrafluoroborate in water 16 h; Ambient temperature;
参考文献
Ranu, Brindaban C.; Jana, Umasish; Majee, Adinath
Tetrahedron Letters, 1999 , vol. 40, # 10 p. 1985 - 1988
反应条件
1H-imidazole in N,N-dimethyl-formamide
T=20°C; silylation; 18 h;
参考文献
Dinsmore, Christopher J.; Zartman, C. Blair; Baginsky, Walter F.; O'Neill, Timothy J.; Koblan, Kenneth S.; Chen, I-Wu; McLoughlin, Debra A.; Olah, Timothy V.; Huff, Joel R.
Organic Letters, 2000 , vol. 2, # 22 p. 3473 - 3476
反应条件
in dichloromethane
T=0 - 20°C; 3 h; Inert atmosphere;
参考文献
Ayala, Caitlan E.; Villalpando, Andres; Nguyen, Alex L.; McCandless, Gregory T.; Kartika, Rendy
Organic Letters, 2012 , vol. 14, # 14 p. 3676 - 3679
反应条件
sodium iodide in acetone
12 h; Reflux;
参考文献
Zhou, Shiqiang; Jia, Yanxing
Organic Letters, 2014 , vol. 16, # 12 p. 3416 - 3418