叔丁基(4-氯丁氧基)二甲基硅烷合成路线 (共 4 条)
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane
T=0 - 20°C; Substitution;
参考文献
Hanson, Ronald L.; Schwinden, Mark D.; Banerjee, Amit; Brzozowski, David B.; Chen, Bang-Chi; Patel, Bharat P.; McNamee, Clyde G.; Kodersha, Gus A.; Kronenthal, David R.; Patel, Ramesh N.; Szarka, Laszlo J.
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 10 p. 2247 - 2252
反应条件
chlorodimethyl(phenylthio)chloride methanaminium in dichloromethane
T=20°C; Chlorination; 3 h;
参考文献
Gomez; Gellibert; Wagner; Mioskowski
Tetrahedron Letters, 2000 , vol. 41, # 32 p. 6049 - 6052
参考文献
Leo Pharmaceutical Products Ltd. A/S Kemiske Fabrik Produkionsaktiese SKAB
Patent: US5401732 A1, 1995 ;
反应条件
triethylamine in dichloromethane
参考文献
Spino, Claude; Liu, Gang; Tu, Noah; Girard, Suzanne
Journal of Organic Chemistry, 1994 , vol. 59, # 19 p. 5596 - 5608