triethylaluminum in hexane; dichloromethane T=-78 - 0°C; 0.333333 h; Product distribution; Further Variations:Temperatures;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />T=0&deg;C;&nbsp;<br /> &nbsp;

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<b>Multi-step reaction with 2 steps<br /> </b>1: 85 percent / tetrahydrofuran / 0.08 h / -78 &deg;C<br />2: Et₃N / CH₂Cl₂ / 0.17 h / 0 &deg;C<br /> <br /> &nbsp;