Begley, Michael J.; Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Osborne, Steven; Webster, Richard A. B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2027 - 2046
Begley, Michael J.; Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Osborne, Steven; Webster, Richard A. B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2027 - 2046
Crombie, Leslie; Jones, Raymond C. F.; Osborne, Steven; Mat-Zin, Ab. Rasid
Journal of the Chemical Society, Chemical Communications, 1983 , # 17 p. 959 - 960
1: 94 percent / KOH, Bu4NHSO4 / tetrahydrofuran / 20 °C
2: 85 percent / 96 h / 45 °C / sealed tube
View Scheme
参考文献
Crombie, Leslie; Jones, Raymond C. F.; Osborne, Steven; Mat-Zin, Ab. Rasid
Journal of the Chemical Society, Chemical Communications, 1983 , # 17 p. 959 - 960
1: 80 percent / diethyl ether / 1 h / Ambient temperature
2: 88 percent / 25percent aq. sodium sulfite, 10percent aq. KOH / diethyl ether; CHCl3 / 1 h
3: 97 percent / tetrabutylammonium hydrogen sulfate, KOH / tetrahydrofuran / 5 h / Ambient temperature
4: 75 percent / 168 h / Ambient temperature
View Scheme
参考文献
Begley, Michael J.; Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Osborne, Steven; Webster, Richard A. B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2027 - 2046
1: 88 percent / 25percent aq. sodium sulfite, 10percent aq. KOH / diethyl ether; CHCl3 / 1 h
2: 97 percent / tetrabutylammonium hydrogen sulfate, KOH / tetrahydrofuran / 5 h / Ambient temperature
3: 75 percent / 168 h / Ambient temperature
View Scheme
参考文献
Begley, Michael J.; Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Osborne, Steven; Webster, Richard A. B.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2027 - 2046