2,3,4,5-四甲氧基-6-甲基苯甲醛合成路线 (共 5 条)
反应条件
titanium tetrachloride in dichloromethane
4 h; Ambient temperature;
参考文献
Ohkawa, Shigenori; Terao, Shinji; Terashita, Zen-ichi; Shibouta, Yumiko; Nishikawa, Kohei
Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 267 - 276
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane in water; trifluoroacetic acid
参考文献
Nisshin Flour Milling Co., Ltd.
Patent: US5756475 A1, 1998 ;
US 5756475 A
反应条件
1: H2 / Pd/C / methanol / 1551.44 - 2327.17 Torr
2: NaOH / methanol
3: TiCl4 / CH2Cl2
View Scheme
参考文献
Jung, Young-Sik; Joe, Bo-Young; Cho, Sung Ju; Konishi, Yasuo
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 4 p. 1125 - 1129
反应条件
1: NaOH / methanol
2: TiCl4 / CH2Cl2
View Scheme
参考文献
Jung, Young-Sik; Joe, Bo-Young; Cho, Sung Ju; Konishi, Yasuo
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 4 p. 1125 - 1129
反应条件
1: NaBH4 / ethanol / 0.5 h / 0 °C
2: PBr3 / tetrahydrofuran / 0.5 h / 0 °C
View Scheme
参考文献
Ma, Wei; Li, Da-Wei; Sutherland, Todd C.; Li, Yang; Long, Yi-Tao; Chen, Hong-Yuan
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12366 - 12369