2-氨基-5-氯-N,3-二甲基苯甲酰胺合成路线 (共 13 条)
反应条件
1.1: sulfuric acid / 0.33 h / 80 °C 2.1: dihydrogen peroxide; sodium hydroxide / water / 0 - 50 °C 3.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.67 h / 100 °C 4.1: thionyl chloride / 3 h / |Reflux 4.2: 20 °C / |Cooling with ice View Scheme
参考文献
Chinese Journal of Chemistry, , vol. 30, # 8 p. 1748 - 1758
反应条件
1.1: dihydrogen peroxide; sodium hydroxide / water / 0 - 50 °C 2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 0.67 h / 100 °C 3.1: thionyl chloride / 3 h / |Reflux 3.2: 20 °C / |Cooling with ice View Scheme
参考文献
Chinese Journal of Chemistry, , vol. 30, # 8 p. 1748 - 1758
参考文献
Journal of Agricultural and Food Chemistry, , vol. 58, # 23 p. 12327 - 12336
Journal of Agricultural and Food Chemistry, , vol. 60, # 31 p. 7565 - 7572