4-(苯磺酰基氨基)苯甲酸乙酯合成路线 （共 7 条）
反应条件
methanol; sodium hydroxide in tetrahydrofuran T=20°C;
参考文献
Zheng, Can-Hui; Yang, Hui; Zhang, Meng; Lu, Shi-Hai; Shi, Duo; Wang, Juan; Chen, Xiu-Hua; Ren, Xiao-Hui; Liu, Jia; Lv, Jia-Guo; Zhu, Ju; Zhou, You-Jun
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 39 - 44
反应条件
1: With pyridine
18 h;
2: With ammonia in methanol
T=90°C; 0.5 h; Microwave irradiation;
参考文献
EVOTEC AG; TAYLOR, Steven; HALLETT, David James; TOWNSEND, Robert James
Patent: WO2010/130638 A1, 2010 ;
Location in patent: Page/Page column 66 ;
WO 2010/130638 A1
反应条件
potassium phosphate; copper(l) iodide; N-methyl-glycine in N,N-dimethyl-formamide
T=100°C; 24 h;
参考文献
Deng, Wei; Liu, Lei; Zhang, Chen; Liu, Min; Guo, Qing-Xiang
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7295 - 7298
反应条件
benzenesulfonyl chloride in pyridine
参考文献
BASF Aktiengesellschaft
Patent: US6251917 B1, 2001 ;
US 6251917 B1
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
T=20°C;
参考文献
Zheng, Can-Hui; Yang, Hui; Zhang, Meng; Lu, Shi-Hai; Shi, Duo; Wang, Juan; Chen, Xiu-Hua; Ren, Xiao-Hui; Liu, Jia; Lv, Jia-Guo; Zhu, Ju; Zhou, You-Jun
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 39 - 44
反应条件
pyridine
24 h; Ambient temperature;
参考文献
Yasuhara, Akito; Kameda, Mitsuyoshi; Sakamoto, Takao
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 6 p. 809 - 812
反应条件
2,6-dimethylpyridine in acetone
Reflux;
参考文献
Fauber, Benjamin P.; De Leon Boenig, Gladys; Burton, Brenda; Eidenschenk, Celine; Everett, Christine; Gobbi, Alberto; Hymowitz, Sarah G.; Johnson, Adam R.; Liimatta, Marya; Lockey, Peter; Norman, Maxine; Ouyang, Wenjun; Rene, Olivier; Wong, Harvey
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6604 - 6609
