3-(4-硝基-苯基)-2,4-戊二酮合成路线 （共 5 条）
反应条件
caesium carbonate; copper(II) oxide in dimethyl sulfoxide
T=80°C; P=760.051 Torr; 6 h; Inert atmosphere;
参考文献
Kidwai, Mazaahir; Bhardwaj, Saurav; Poddar, Roona
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 35
反应条件
in dimethyl sulfoxide
T=25°C; 5 h;
参考文献
Dell'Erba; Novi; Petrillo; Tavani; Bellandi
Tetrahedron, 1991 , vol. 47, # 2 p. 333 - 342
反应条件
boron trifluoride diethyl etherate in diethyl ether
T=0°C; 4 h;
参考文献
Emsley, John; Ma, Lewina Y. Y.; Bates, Paul A.; Motevalli, Majid; Hurtshouse, Michael B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 527 - 534
反应条件
copper acetylacetonate; copper
T=40°C; 0.5 h;
参考文献
Citterio, Attilio; Ferrario, Francesco
Journal of Chemical Research, Miniprint, 1983 , # 12 p. 2656 - 2668
反应条件
1: K-tert-butoxide / dimethylsulfoxide / cooling
2: 72 percent / dimethylsulfoxide / 5 h / 25 °C
View Scheme
参考文献
Dell'Erba; Novi; Petrillo; Tavani; Bellandi
Tetrahedron, 1991 , vol. 47, # 2 p. 333 - 342
