2-氯-3-(2-甲基苯基)喹唑啉-4(3H)-酮合成路线 （共 5 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); PivNHOH; sodium carbonate in chlorobenzene T=120°C; Inert atmosphere;
参考文献
Tsukano, Chihiro; Okuno, Masataka; Nishiguchi, Hiromi; Takemoto, Yoshiji
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1533 - 1538
反应条件
1: triethylamine / 1,2-dichloro-ethane / 2 h / |Reflux
2: pyridine / tetrahydrofuran / |Reflux
3: sodium ethanolate / ethanol / |Reflux
4: trichlorophosphate / 48 h / |Reflux
View Scheme
参考文献
Tsukano, Chihiro; Okuno, Masataka; Nishiguchi, Hiromi; Takemoto, Yoshiji
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1533 - 1538
反应条件
1: pyridine / tetrahydrofuran / |Reflux
2: sodium ethanolate / ethanol / |Reflux
3: trichlorophosphate / 48 h / |Reflux
View Scheme
参考文献
Tsukano, Chihiro; Okuno, Masataka; Nishiguchi, Hiromi; Takemoto, Yoshiji
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1533 - 1538
反应条件
1: sodium ethanolate / ethanol / |Reflux
2: trichlorophosphate / 48 h / |Reflux
View Scheme
参考文献
Tsukano, Chihiro; Okuno, Masataka; Nishiguchi, Hiromi; Takemoto, Yoshiji
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1533 - 1538
反应条件
trichlorophosphate
48 h; Reflux;
参考文献
Tsukano, Chihiro; Okuno, Masataka; Nishiguchi, Hiromi; Takemoto, Yoshiji
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1533 - 1538
