in neat (no solvent) byproducts: H2; (N2), Schlenk techniques; heating Sn compd. (200°C) under reducedpressure (1E-3 mm Hg) for 6 h or sealing Sn compd. under reduced pressu re (5E-1 mm Hg) with heating (200°C) for 4 h; isolation of crystals, NMR;
参考文献
Canadian Journal of Chemistry, , vol. 88, # 10 p. 1046 - 1052
in neat (no solvent) byproducts: H2; (N2), Schlenk techniques; sealing mixture of Bu3SnH and Ph3SnH under reduced pressure (5E-1 mm Hg), heating (200°C) for 5 h; NMR;
参考文献
Canadian Journal of Chemistry, , vol. 88, # 10 p. 1046 - 1052
(C2H5)3N in not given formation at 20°C after 25 h;;
参考文献
Neumann, W. P.; Schneider, B.; Sommer, R.
Liebigs Annalen der Chemie, 1966 , vol. 692, p. 1 - 11
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.1.1.5, page 41 - 43
