2,2'-azobisisobutyronitrile in melt
(N2); heating a melt of tin compd. with ligand and AIBN to 140°C for 1 h; cooling, column chromy. (SiO2, gradient petroleum ether/CH2Cl2); elem. anal.;
参考文献
Deacon; Devylder; Hill; Mahon; Molloy; Price
Journal of Organometallic Chemistry, 2003 , vol. 687, # 1 p. 46 - 56
2,2'-azobisisobutyronitrile in melt
(N2); heating a melt of tin compd. with ligand and AIBN to 140°C for 1 h; cooling, column chromy. (SiO2, gradient petroleum ether/CH2Cl2); elem. anal.;
参考文献
Deacon; Devylder; Hill; Mahon; Molloy; Price
Journal of Organometallic Chemistry, 2003 , vol. 687, # 1 p. 46 - 56
2,2'-azobisisobutyronitrile in melt
(N2); heating a melt of tin compd. with ligand and AIBN to 140°C for 1 h; cooling, column chromy. (SiO2, gradient petroleum ether/CH2Cl2); elem. anal.;
参考文献
Deacon; Devylder; Hill; Mahon; Molloy; Price
Journal of Organometallic Chemistry, 2003 , vol. 687, # 1 p. 46 - 56
2,2'-azo-bisisobutyronitrile in neat (no solvent)
under protective gas addn. of AIBN to the mixt. of (C6H5)3SnH and P(C6H5)2CHCH2 without solvent, slowly heating to 60-70°C, then 6-7 h at 70-90°C meanwhile addn. of the rest of AIBN; recrystn. from hexane, elem. anal.;
参考文献
Weichmann, H.; Quell, G.; Tzschach, A.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1980 , vol. 462, p. 7 - 17
